Microstructural Analysis and Machine Learning-Based Prediction of Polymer-Modified Soil Characteristics
Received: 20 May 2025 | Revised: 11 June 2025 | Accepted: 28 June 2025 | Online: 2 August 2025
Corresponding author: Aliya K. Aldungarova
Abstract
The use of polymers in geotechnical engineering has accelerated rapidly due to their ability to enhance the mechanical and physical properties of soils. However, despite increasing interest, predicting the behavior of such materials across varying polymer concentrations remains a challenge and requires additional tools for an accurate evaluation. This study presents an integrated approach to the analysis and prediction of microstructural changes in polymer-modified soils that combines microscopy techniques with machine learning methods. A detailed microstructural analysis was conducted on soils modified with Xanthan Gum (XG) and Carboxymethyl Cellulose (CMC) using Scanning Electron Microscopy (SEM), Energy-Dispersive X-ray Spectroscopy (EDS), and elemental and morphological heatmap visualizations. These techniques allowed for a comprehensive investigation of microlevel changes occurring due to varying polymer concentrations. Based on experimental data, a linear regression model was developed to predict microstructural characteristics at a polymer concentration of 12%, an untested level in the laboratory. The results show that machine learning-based predictions derived from experimental data at lower concentrations (3%, 6%, and 9%) can effectively estimate microstructural parameters at higher concentrations. This approach offers a cost-effective and time-saving solution for the development of new and sustainable soil modification strategies. The optimized soil-to-polymer ratio is key to consistent microstructural modification.
Keywords:
polymer, soil, microstructural analysis, machine learning, morphologyDownloads
References
A. Sagybekova, S. Kiyalbay, A. Belov, A. Kiyalbayev, and K. Tursumbekova, "Comparison of test results to determine the parameters of soil strength to ensure the stability of earth slopes," EUREKA: Physics and Engineering, no. 6, pp. 3–11, Nov. 2022. DOI: https://doi.org/10.21303/2461-4262.2022.002691
M. Otieno, C. Kabubo, and Z. Gariy, "Mechanical and Structural Correlation of Lateritic Soil Road Base Stabilized with Cement and Selected Biochars," Engineering, Technology & Applied Science Research, vol. 13, no. 4, pp. 11070–11077, Aug. 2023. DOI: https://doi.org/10.48084/etasr.5973
A. Tulebekova, "A Practical Solution for Improving Soil Bases in Problematic Engineering Conditions," International Journal of GEOMATE, vol. 25, no. 108, Aug. 2023. DOI: https://doi.org/10.21660/2023.108.3849
A. Lakirouhani, M. Abbasian, J. Medzvieckas, and R. Kliukas, "The effect of relative density, granularity and size of geogrid apertures on the shear strength of the soil/geogrid interface," Journal of Civil Engineering and Management, vol. 30, no. 8, pp. 691–707, Sep. 2024. DOI: https://doi.org/10.3846/jcem.2024.22236
L. Z. Wongbae, C. Kabubo, and A. Owayo, "The Effect of Waste Marble Dust and Corncob Ash on the Engineering and Micro-Structural Properties of Expansive Soil for Use in Road Subgrades," Engineering, Technology & Applied Science Research, vol. 14, no. 2, pp. 13765–13772, Apr. 2024. DOI: https://doi.org/10.48084/etasr.7034
A. Tulebekova, Z. Kusbergenova, B. Dosmukhambetova, T. Abilmazhenov, and I. Zhumadilov, "Study of the impact of biopolymer and geosynthetics reinforcement on soil strengthening," EUREKA: Physics and Engineering, no. 6, pp. 70–80, Nov. 2024. DOI: https://doi.org/10.21303/2461-4262.2024.003472
L. Xu, X. Wang, Y. Qi, C. Yuan, Z. Ding, and R. Xu, "Strength Model for Cement-Stabilized Marine Clay: SEM Image Analysis and Microstructural Insights," Journal of Marine Science and Engineering, vol. 13, no. 2, Feb. 2025, Art. no. 388. DOI: https://doi.org/10.3390/jmse13020388
Q. Chen, R. Yu, T. Gaoliang, and S. Nimbalkar, "Microstructure, strength and durability of nano-cemented soils under different seawater conditions: laboratory study," Acta Geotechnica, vol. 18, no. 3, pp. 1607–1627, Mar. 2023. DOI: https://doi.org/10.1007/s11440-022-01688-1
Q. O. Babatunde and Y. H. Byun, "Soil Stabilization Using Zein Biopolymer," Sustainability, vol. 15, no. 3, Jan. 2023, Art. no. 2075. DOI: https://doi.org/10.3390/su15032075
J. Wan, Z. Tang, Y. Liu, H. Xiao, and H. Wang, "Study on the improvement of clay properties by xanthan gum and its application on ecological slope protection engineering," Environmental Technology, vol. 45, no. 14, pp. 2762–2775, Jun. 2024. DOI: https://doi.org/10.1080/09593330.2023.2186271
N. Hataf, P. Ghadir, and N. Ranjbar, "Investigation of soil stabilization using chitosan biopolymer," Journal of Cleaner Production, vol. 170, pp. 1493–1500, Jan. 2018. DOI: https://doi.org/10.1016/j.jclepro.2017.09.256
S. Smitha and A. Sachan, "Use of agar biopolymer to improve the shear strength behavior of sabarmati sand," International Journal of Geotechnical Engineering, vol. 10, no. 4, pp. 387–400, Aug. 2016. DOI: https://doi.org/10.1080/19386362.2016.1152674
Y. Trambitski, O. Kizinievič, and V. Kizinievič, "Effect of Modified Starch on Properties of Clay Composites," Materials Science Forum, vol. 1071, pp. 215–221, Oct. 2022. DOI: https://doi.org/10.4028/p-x5735l
Y. Xi, M. Sun, H. Li, G. Li, P. Wang, and L. Li, "Permeability and Disintegration Characteristics of Loess Solidified by Guar Gum and Basalt Fiber," Materials, vol. 17, no. 13, Jun. 2024, Art. no. 3150. DOI: https://doi.org/10.3390/ma17133150
"GOST 5180: Soils. Laboratory methods for the determination of physical characteristics." Federal Agency for Technical Regulation and Metrology, Russia, 2015.
"GOST 25100: Soils. Classification." Federal Agency for Technical Regulation and Metrology, Russia, 2020.
S. J. Armistead, C. C. Smith, and S. S. Staniland, "Sustainable biopolymer soil stabilisation: the effect of microscale chemical characteristics on macroscale mechanical properties," Acta Geotechnica, vol. 18, no. 6, pp. 3213–3227, Jun. 2023. DOI: https://doi.org/10.1007/s11440-022-01732-0
S. Selvakumar, B. Soundara, N. Raj, and P. Kulanthaivel, "Microstructural investigation on the expansive soils for sustainable stabilization purposes," Discover Soil, vol. 1, no. 1, Sep. 2024, Art. no. 8. DOI: https://doi.org/10.1007/s44378-024-00009-0
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Copyright (c) 2025 Assel S. Tulebekova, Zhanar T. Kusbergenova, Atogali A. Jumabayev, Aliya K. Aldungarova, Talgat Akhmetzhanov

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